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Properties of substance:
trifluoroacetic acid
Group of substances:
organic
Physical appearance:
colorless fuming liquid
Empirical formula (Hill's system for organic substances):
C
2
HF
3
O
2
Structural formula as text:
CF3COOH
Molar/atomic mass: 114.03
Melting point (°C):
-15.36
Boiling point (°C):
72.4
Solubility (g/100 g of solvent):
acetone
: soluble [
Ref.
]
diethyl ether
: soluble [
Ref.
]
ethanol
: soluble [
Ref.
]
hydrogen fluoride
: miscible [
Ref.
]
water
: very soluble [
Ref.
]
Density:
1.53514 (0°C, g/cm
3
)
1.489 (20°C, d
4
)
Reactions of synthesis:
Yeild 84-90%. [
Ref.1
]
3CF
3
CCl=CCl
2
+ 4KMnO
4
+ 14KOH → 3CF
3
COOK + 4MnO
2
+ 9KCl + 3K
2
CO
3
+ 7H
2
O
CF
3
COOK + H
2
SO
4
→ CF
3
COOH + KHSO
4
Refractive index (n
D
):
1.285 (20°C)
Dissociation:
H
0
(1) = -3.1 (25°C)
pK
a
(1) = 0.23 (25°C, water)
pK
a
(1) = 5.4 (25°C, acetic acid)
Permittivity (dielectric constant):
8.55 (20°C)
Viscosity (mPa·s):
0.876 (20°C)
1.225 (0°C)
Standard molar enthalpy (heat) of formation Δ
f
H
0
(298.15 K, kJ/mol):
-1020 (l)
Enthalpy (heat) of vaporization Δ
vap
H (kJ/mol):
34.21
Standard molar enthalpy (heat) of formation Δ
f
H
0
(298.15 K, kJ/mol):
-1031.4 (g)
Critical temperature (°C):
218.15
Critical pressure (MPa):
3.26
Critical density (g/cm
3
):
0.525
References:
CRC Handbook of Chemistry and Physics. - 90ed. - CRC Press, 2010. - pp. 5-21
Альберт А., Сержент Е. Константы ионизации кислот и оснований. - М.-Л.: Химия, 1964. - pp. 118 [Russian]
Гудлицкий М. Химия органических соединений фтора. - М.: ГНТИХЛ, 1961. - pp. 270 [Russian]
Краткая химическая энциклопедия. - Т. 5: Т-Я. - М.: Советская энциклопедия, 1967. - pp. 276 [Russian]
Некрасов Б.В. Основы общей химии. - Т.1. - М.: Химия, 1973. - pp. 563-564 [Russian]
Промышленные фторорганические продукты: Справочник. - Л.: Химия, 1990. - pp. 367-371 [Russian]
Рабинович В.А., Хавин З.Я. Краткий химический справочник. - Л.: Химия, 1977. - pp. 184 [Russian]
Справочник химика. - Т. 3. - М.-Л.: Химия, 1965. - pp. 118 [Russian]
Фтор и его соединения. – Под ред. Саймонса Дж., Т. 2. - М.: ИИЛ, 1956. - pp. 357 [Russian]
Химическая энциклопедия. - Т. 5. - М.: Советская энциклопедия, 1999. - pp. 9 [Russian]
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© Collected Ruslan Anatolievich Kiper, burewestnik@mail.ru